1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
in tetrahydrofuran
1) 3,7 h, T < 38 deg C 2) 1 h, to -15 to -10 deg C;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
反应条件
dioxochloro(trimethylsiloxy)chromate(VI); iodine in dichloromethane
T=0°C; 1.25 h;
参考文献
Aizpurua, J. M.; Juaristi, M.; Lecea, B.; Palomo, C.
Tetrahedron, 1985 , vol. 41, # 14 p. 2903 - 2912
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=130°C; Heck reaction; 20 h;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
pyridine
T=0°C; 2 h;
参考文献
Sakakura, Toshiyasu; Hara, Masayasu; Tanaka, Masato
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 3 p. 283 - 288
反应条件
titanium tetrachloride in dichloromethane
T=-78°C;
参考文献
Kobayashi, Shu; Murakami, Masahiro; Mukaiyama, Teruaki
Chemistry Letters, 1985 , p. 953 - 956
反应条件
[VO(OEt)Cl2] in dichloromethane
1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
1: CH2Cl2 / -78 °C
2: 40 percent Chromat. / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
反应条件
1: With lithium boron tetrafluoride; [Ru(2,2′-bipyridine)3][hexafluorophosphate]2; 2,3,5,6-tetramethyl-p-benzoquinone in aceonitrile
T=20°C; 5 h; Inert atmosphereIrradiationMolecular sieve;
2: With water; ammonium chloride in acetonitrile
T=20°C; 1 h; Inert atmosphereMolecular sieve; optical yield given as percent de;
参考文献
Yasu, Yusuke; Koike, Takashi; Akita, Munetaka
Chemical Communications, 2012 , vol. 48, # 43 p. 5355 - 5357
反应条件
in diethyl ether
T=-78 - 20°C;
参考文献
Prasad; Para; Tummino; Ferguson; McQuade; Lunney; Rapundalo; Batley; Hingorani; Domagala; Gracheck; Bhat; Liu; Baldwin; Erickson; Sawyer
Journal of Medicinal Chemistry, 1995 , vol. 38, # 6 p. 898 - 905
反应条件
zinc(II) chloride in ethyl acetate
T=40 - 45°C; 0.5 h;
参考文献
Amerkhanov, R. R.; Musavirov, R. S.; Rakhmankulov, D. L.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 4.2 p. 610 - 613
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 4 p. 573 - 575
