1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
zinc(II) chloride in ethyl acetate
T=40 - 45°C; 1 h;
参考文献
Amerkhanov, R. R.; Musavirov, R. S.; Rakhmankulov, D. L.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 4.2 p. 610 - 613
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 4 p. 573 - 575
反应条件
trimethylsilyl iodide in acetonitrile
0.5 h; Ambient temperature;
参考文献
Hosomi, Akira; Sakata, Yasuyuki; Sakurai, Hideki
Chemistry Letters, 1983 , p. 405 - 408
反应条件
zinc dibromide in dichloromethane
1 h; Ambient temperature;
参考文献
Shimagaki, Masayuki; Suzuki, Atsushi; Nakata, Tadashi; Oishi, Takeshi
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 8 p. 3138 - 3141
反应条件
dodecacarbonyltetrarhodium(0) in benzene
T=100°C; 15 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
反应条件
1: 1.) TiCl4 / 1) CH2Cl2, -78 deg C, 1 min; 2) CH2Cl2, -78 deg C, 3 h
2: Et3N / CH2Cl2 / 1) 0 deg C, 10 min; 2) 0 deg C --> rt, 1 h
3: 70 percent / DBU / benzene / 1.5 h / Ambient temperature
View Scheme
参考文献
Arai, Noriyoshi; Narasaka, Koichi
Chemistry Letters, 1995 , # 11 p. 987 - 988
反应条件
titanium tetrachloride; triethylamine; trifluoroacetic anhydride
Yield given. Multistep reaction;
参考文献
Bouhlel; Hassine
Synthetic Communications, 1992 , vol. 22, # 15 p. 2183 - 2186
反应条件
water; cesium fluoride
1.) 100 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Boyer, J.; Corriu, R. J. P.; Perz, R.; Reye, C.
Journal of Organometallic Chemistry, 1980 , vol. 184, # 2 p. 157 - 166
反应条件
1: With trifluorormethanesulfonic acid in acetonitrile
T=20°C; 3 h;
2: With manganese triacetate in acetic acid; acetonitrile
T=20°C; 24 h;
参考文献
Akiyama, Takahiko; Nakashima, Saeko; Yokota, Koji; Fuchibe, Kohei
Chemistry Letters, 2004 , vol. 33, # 7 p. 922 - 923
反应条件
perchloric acid in acetonitrile
T=20°C;
参考文献
Akiyama, Takahiko; Nakashima, Saeko; Yokota, Koji; Fuchibe, Kohei
Chemistry Letters, 2004 , vol. 33, # 7 p. 922 - 923
反应条件
tert.-butylhydroperoxide; copper(I) bromide in decane; acetonitrile
T=20 - 50°C; in air; regiospecific reaction;
参考文献
Huang, Lehao; Zhang, Xunbin; Zhang, Yuhong
Organic Letters, 2009 , vol. 11, # 16 p. 3730 - 3733
