1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Journal of Organometallic Chemistry, , vol. 153, p. 137 - 151
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
trimethylsilyl trifluoromethanesulfonate T=0°C; 27 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 17 p. 1268 - 1270
反应条件
in tetrahydrofuran; dimethyl-ether T=-135°C; other mol ratio and temperature; Product distribution;
参考文献
Tetrahedron Letters, , vol. 24, # 45 p. 4907 - 4910
反应条件
in tetrahydrofuran 1 h; -70 --> 25 deg C;
参考文献
Tetrahedron Letters, , vol. 30, # 15 p. 1975 - 1978
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane Heating;
参考文献
Liebigs Annalen der Chemie, , # 6 p. 607 - 614
反应条件
trifluorormethanesulfonic acid; triethylamine 1) CH2Cl2, ice colling to r.t., 15 to 20 min, 2) CH2Cl2; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 5212 - 5214
反应条件
1.) THF, diethyl ether, pentane, hexane, -110 +/- 5 deg C, 2.) 2h, -110 deg C, 3.) 1h, 4.) 1h, RT; Yield given. Multistep reaction;
参考文献
Seyferth, Dietmar; Weinstein, Robert M.; Wang, Wei-Liang
Journal of Organic Chemistry, 1983 , vol. 48, # 7 p. 1144 - 1146
参考文献
Journal of Organometallic Chemistry, , vol. 66, p. 29 - 41
反应条件
carbon monoxide 1.) THF, diethyl ether, pentane, -110 deg C, 2 h, 2.) -110 deg C to r.t, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 57, # 21 p. 5620 - 5629
