1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=130°C; Heck reaction; 20 h;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
反应条件
ZnF2; tri-tert-butyl phosphine; cesium fluoride; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=70°C; Product distribution; Further Variations:Reagents;
参考文献
Su, Weiping; Raders, Steven; Verkade, John G.; Liao, Xuebin; Hartwig, John F.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 35 p. 5852 - 5855
反应条件
silica gel
1.) 110 deg C, 15 h, 2.) CHCl3, r.t., 20 h; Multistep reaction. Yields of byproduct given;
参考文献
Lociuro, Sergio; Pellacani, Lucio; Tardella, Paolo A.
Tetrahedron Letters, 1983 , vol. 24, # 6 p. 593 - 596
反应条件
bis-(trifluoromethylsulphonyl)amine in acetonitrile
T=20°C;
参考文献
Devineau, Alice; Pousse, Guillaume; Taillier, Catherine; Blanchet, Jerome; Rouden, Jacques; Dalla, Vincent
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2881 - 2886
反应条件
ytterbium(III) triflate in dichloromethane
16 h; Ambient temperature;
参考文献
Kobayashi; Hachiya; Takahori
Synthesis, 1993 , # 4 p. 371 - 373
反应条件
hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; diethylaluminium chloride
1.) CH2Cl2, -78 deg C, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Oishi; Aratake; Yamamoto
Journal of the American Chemical Society, 1998 , vol. 120, # 32 p. 8271 - 8272
反应条件
1: CH2Cl2 / -78 °C
2: 42 percent Chromat. / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
反应条件
in dichloromethane
0.166667 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
反应条件
1: CH2Cl2 / -78 °C
2: 34 percent Chromat. / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
反应条件
in dichloromethane
0.166667 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
