1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
tin(IV) chloride in dichloromethane
T=-78°C; 0.5 h;
参考文献
Meanwell, Nicholas A.; Johnson, Carl R.
Synthesis, 1982 , # 4 p. 283 - 284
反应条件
(i) PCl5, benzene, (ii) SO2; Multistep reaction;
参考文献
Lazukina,L.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, # 9 p. 2006 - 2011,1931 - 1935
反应条件
solid acid of tin(IV) ion-exchanged montmorillonite in dichloromethane
T=0°C; Mukaiyama Aldol Addition; 0.75 h; Inert atmosphere; Reagent/catalystTemperature;
参考文献
Takehira, Satoshi; Masui, Yoichi; Onaka, Makoto
Chemistry Letters, 2014 , vol. 43, # 4 p. 498 - 500
反应条件
bismuth trifluoromethanesulphonate in nitromethane
T=20°C; 3 h;
参考文献
Rubenbauer, Philipp; Bach, Thorsten
Tetrahedron Letters, 2008 , vol. 49, # 8 p. 1305 - 1309
反应条件
potassium hydroxide; ammonium cerium(IV) nitrate in methanol
T=-78°C; Alkylation; 0.25 h;
参考文献
Arai, Noriyoshi; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 10 p. 2525 - 2534
反应条件
iodosylbenzene in dichloromethane
-78 deg C to room temp. 2.5 h;
参考文献
Moriarty, Robert M.; Epa, W. Ruwan; Penmasta, Raju; Awasthi, Alok K.
Tetrahedron Letters, 1989 , vol. 30, # 6 p. 667 - 670
参考文献
Zhdankin, Viktor V.
Tetrahedron Letters, 1990 , vol. 31, # 34 p. 4821 - 4824
反应条件
trimethylsilyl cyanide; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in acetonitrile
3 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Soga, Tsunehiko; Takenoshita, Haruhiro
Chemistry Letters, 1989 , p. 1273 - 1276
反应条件
lithium perchlorate; sodium carbonate in acetonitrile
Yields of byproduct given;
参考文献
Renaud, Roger N.; Stephens, Campbell J.; Brochu, Gaetan
Canadian Journal of Chemistry, 1984 , vol. 62, p. 565 - 569
反应条件
in toluene
T=100°C; 1 h;
参考文献
Saitoh; Oyama; Sakurai; Niimura; Hinata; Horiguchi; Toda; Sano
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 5 p. 956 - 966
