1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
in chloroform-d1 2.5 h; Ambient temperaturesonication;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, p. 3649 - 3652
反应条件
tetraphenyl stibonium bromide; N-phenyl-azilidine 1.) CH2Cl2, r.t., 5 min; 2.) 40 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Chemistry Letters, , p. 1247 - 1250
反应条件
(K-18-crown-6 ether) cyanide in tetrahydrofuran T=20°C; 8 h; Equilibrium constant;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 34, # 11 p. 2396 - 2399
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2585 - 2589
反应条件
lithium diisopropyl amide 1) -78 deg C, THF, 2) in 6 h to 0 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 123, # 1 p. 107 - 114
反应条件
(i) tBuLi, THF, ether, pentane, (ii) /BRN= 1739972/; Multistep reaction;
参考文献
Chemische Berichte, , vol. 111, p. 2785 - 2812
反应条件
[Ru(N,N'-ethylenebis(salicylideneaminate)(NO)(H2O)](SbF6) in CD3NO2 T=25°C; 0.5 h;
参考文献
Hollis, T. Keith; Odenkirk, William; Robinson; Whelan, John; Bosnich
Tetrahedron, 1993 , vol. 49, # 25 p. 5415 - 5430
反应条件
water; indium(III) chloride T=20°C; Mukaiyama-type addition; 0.833333 h;
参考文献
Chancharunee, Sirirat; Perlmutter, Patrick; Statton, Maya
Tetrahedron Letters, 2003 , vol. 44, # 30 p. 5683 - 5685
反应条件
in dichloromethane; hexafluoroisopropyl alcohol T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Ratnikov, Maxim O.; Tumanov, Vasily V.; Smit, William A.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 50 p. 9739 - 9742
反应条件
aluminosilicates, mesoporous in dichloromethane T=30°C; Mukaiyama reaction; 0.25 h;
参考文献
Ito, Suguru; Yamaguchi, Hitoshi; Kubota, Yoshihiro; Asami, Masatoshi
Chemistry Letters, 2009 , vol. 38, # 7 p. 700 - 701
反应条件
1: boron trifluoride-diethyl etherate / CH2Cl2 / -78 °C 2: 40 percent / electrolytic manganese dioxide; air / hexane / 3 h / 20 °C View Scheme
参考文献
Kuroda, Hirofumi; Izawa, Hironori
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 4 p. 780 - 782