1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
lt;Ru(PPh3)3Cl2gt; in benzene T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride 1.) CH2Cl2, room temperature, 10 h, 2.) DMF, room temperature, 24 h; Yield given. Multistep reaction;
参考文献
Matano, Yoshihiro; Azuma, Nagao; Suzuki, Hitomi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1739 - 1748
反应条件
titanium tetrachloride in dichloromethane T=-70°C; 1 h;
参考文献
Mulzer, Johann; Bruentrup, Gisela; Hartz, Georg; Kuehl, Uwe; Blaschek, Ursula; Boehrer, Gerald
Chemische Berichte, 1981 , vol. 114, # 11 p. 3701 - 3724
反应条件
AcOF in chloroform; acetic acid; acetonitrile
参考文献
Journal of Fluorine Chemistry, , vol. 61, # 1.2 p. 141 - 146
反应条件
zinc(II) iodide in diethyl ether 2 h; Ambient temperature;
参考文献
Xu, Yuelian; Dolbier Jr., William R.
Journal of Organic Chemistry, 2000 , vol. 65, # 7 p. 2134 - 2137
反应条件
chloromethyl iodide in dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
Miyano, Sotaro; Hokari, Hiroshi; Mori, Akira; Hashimoto, Harukichi
Chemistry Letters, 1980 , p. 1213 - 1214
反应条件
in chloroform; acetonitrile T=-40 - 20°C;
参考文献
Journal of the American Chemical Society, , vol. 114, # 20 p. 7643 - 7645
反应条件
Ph[I(OH)OTf] 18-crown-6 complex monohydrate T=-78 - 20°C; 7 h;
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 1 p. 75 - 78
反应条件
lead(IV) acetate 2 h; Ambient temperature;
参考文献
Synthetic Communications, , vol. 17, # 6 p. 709 - 714
反应条件
in tetrahydrofuran T=-40 - 20°C; 0.2 h;
参考文献
Ooi, Takashi; Goto, Ryoji; Maruoka, Keiji
Journal of the American Chemical Society, 2003 , vol. 125, # 35 p. 10494 - 10495