1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
in acetonitrile T=0°C; Yield given;
参考文献
Rochin, C.; Babot, O.; Dunogues, J.; Duboudin, F.
Synthesis, 1986 , # 8 p. 667 - 668
反应条件
in anhydrous xylene T=140°C; Diels-Alder reaction; 24 h; regioselective reaction;
参考文献
Anderson, Erin D.; Boger, Dale L.
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 12285 - 12292
反应条件
hydrogen; zinc(II) chloride; palladium dichloride 1.) THF, 25 deg C, 2.) EtOH, 25 deg C, p= 20 psi; Yield given. Multistep reaction;
参考文献
Sinclair, Peter J.; Zhai, Dongguan; Reibenspies, Joseph; Williams, Robert M.
Journal of the American Chemical Society, 1986 , vol. 108, # 5 p. 1103 - 1104
反应条件
silver trifluoroacetate in dichloromethane T=25°C; 0.166667 h;
参考文献
Jefford, Charles W.; Sledeski, Adam W.; Lelandais, Patrick; Boukouvalas, John
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1855 - 1858
反应条件
in dichloromethane T=20°C;
参考文献
Majchrzak, Agnieszka; Mloston, Grzegorz; Linden, Anthony; Heimgartner, Heinz
Helvetica Chimica Acta, 2006 , vol. 89, # 5 p. 1042 - 1061
反应条件
tetrachlorosilane; mercury(II) diacetate in dichloromethane Ambient temperature;
参考文献
Denmark, Scott E.; Stavenger, Robert A.; Winter, Stephen B. D.; Wong, Ken-Tsung; Barsanti, Paul A.
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9517 - 9523
反应条件
scandium tris(trifluoromethanesulfonate) in ethylene glycol dimethyl ether T=-20 - 20°C; Mukaiyama aldol reaction; 6 h; Product distribution; Further Variations:Solvents;
参考文献
Angell, Paul; Zhang, Ji; Belmont, Daniel; Curran, Timothy; Davidson, James G.
Tetrahedron Letters, 2005 , vol. 46, # 12 p. 2029 - 2032
反应条件
titanium tetrachloride in dichloromethane T=-70°C; 1 h;
参考文献
Mulzer, Johann; Bruentrup, Gisela; Hartz, Georg; Kuehl, Uwe; Blaschek, Ursula; Boehrer, Gerald
Chemische Berichte, 1981 , vol. 114, # 11 p. 3701 - 3724
反应条件
scandium tris(trifluoromethanesulfonate) in diethyl ether T=-20 - 18°C; Mukaiyama aldol reaction; 21 h;
参考文献
WARNER-LAMBERT COMPANY LLC
Patent: US2006/4211 A1, 2006 ;
Location in patent: Page/Page column 10 ;
反应条件
carbonyl(η1-0-1-phenyl-1-oxyethyl)lt;bis(trimethylphosphine)gt;rhodium(I) in dimethyl sulfoxide 0.5 h; Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 111, # 3 p. 938 - 949
