1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
water; cesium fluoride 1.) 25 deg C, 45 min, 25 deg C; Yield given. Multistep reaction;
参考文献
Boyer, J.; Corriu, R. J. P.; Perz, R.; Reye, C.
Journal of Organometallic Chemistry, 1980 , vol. 184, # 2 p. 157 - 166
反应条件
chloromethyl methyl ether; tin(ll) chloride in dichloromethane 2 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Miyauchi,Yuka; Koga, Gen
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 12 p. 3716 - 3718
反应条件
1: ammonium hexanitratocerate(IV); KOH / methanol / 0.25 h / -78 °C 2: triethylamine / CH2Cl2 / 20 °C View Scheme
参考文献
Arai, Noriyoshi; Narasaka, Koichi
Chemistry Letters, 1995 , # 11 p. 987 - 988
反应条件
fluorine in chloroform; water; acetonitrile T=0 - 20°C;
参考文献
Dayan, Sharon; Bareket, Yifat; Rozen, Shlomo
Tetrahedron, 1999 , vol. 55, # 12 p. 3657 - 3664
反应条件
18-crown-6 ether; PhIO(1+)*BF4(1-)*18-crown-6 T=-78 - 20°C; 3.5 h;
参考文献
Journal of the American Chemical Society, , vol. 125, # 43 p. 13006 - 13007
反应条件
tert.-butylhydroperoxide; titanium silicate 24 h; Heating;
参考文献
Chemical Communications, , # 16 p. 1969 - 1970
反应条件
tris(cetyl)pyridinium 12-tungstophosphate; dihydrogen peroxide in dichloromethane T=20°C; oxidative cleavage; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 64, # 16 p. 5954 - 5957
反应条件
potassium fluoride; oxygen; isobutyraldehyde; bis(3-methyl-2,4-pentanedionato)nickel(II) 1.) 1,2-dichloroethane, RT, 6 h, 2.) MeOH; Yield given. Multistep reaction;
参考文献
Takai, Toshihiro; Yamada, Tohru; Rhode, Oliver; Mukaiyama, Teruaki
Chemistry Letters, 1991 , # 2 p. 281 - 284
反应条件
1: in ethanol T=20°C; 44 h; 2: With hydrogenchloride in ethanol
参考文献
Armstrong, Alan; Edmonds, Ian D.; Swarbrick, Martin E.; Treweeke, Nigel R.
Tetrahedron, 2005 , vol. 61, # 35 p. 8423 - 8442
反应条件
1: With iodotoluene difluoride; boron trifluoride diethyl etherate in dichloromethane T=-78°C; 2 h; 2: With triethylamine tris(hydrogen fluoride) in dichloromethane 1 h;
参考文献
Synthesis, , # 15 art. no. F18704SS, p. 2602 - 2605
