1-甲氧基-2-(甲基磺酰基)苯合成路线 （共 20 条）
反应条件
aluminum oxide; phosphorus pentoxide
Friedel-Crafts reaction; 1 h; Heating; Title compound not separated from byproducts;
参考文献
Hajipour, Abdol R.; Zarei, Amin; Khazdooz, Leila; Pourmousavi, Seied A.; Mirjalili, Bi Bi F.; Ruoho
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2029 - 2034
反应条件
1: potassium tert-butylate / ethanol / 20 °C
2: oxygen; copper diacetate; silver carbonate / N,N-dimethyl-formamide / 18 h / 145 °C
View Scheme
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9938 - 9941
反应条件
in methanol
T=140°C;
参考文献
Shein,S.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1968 , vol. 4, p. 632 - 636
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 4 p. 648 - 653
反应条件
trifluorormethanesulfonic acid in neat (no solvent)
T=30°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ono, Mitsunori; Nakamura, Yoshisada; Sato, Shingo; Itoh, Isamu
Chemistry Letters, 1988 , p. 395 - 398
反应条件
permanganate(VII) ion
参考文献
Pollard; Robinson
Journal of the Chemical Society, 1926 , p. 3091 Anm.
反应条件
sodium methylate in methanol
T=190°C; Kinetics;
参考文献
Shein,S.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1968 , vol. 4, p. 632 - 636
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 4 p. 648 - 653
参考文献
Holmes; Ingold; Ingold
Journal of the Chemical Society, 1926 , p. 1689
反应条件
(i) NaNO2, aq. HCl, (ii) H3PO2; Multistep reaction;
参考文献
Collins; Davis
Journal of the Chemical Society. Perkin transactions 1, 1966 , vol. 23, p. 2196 - 2201
反应条件
1: (i) aq. NaOAc, acetone, (ii) aq. HCl
2: (i) NaNO2, aq. HCl, (ii) H3PO2
View Scheme
参考文献
Collins; Davis
Journal of the Chemical Society. Perkin transactions 1, 1966 , vol. 23, p. 2196 - 2201
反应条件
1: aq. HBr / Heating
2: Heating
3: AlCl3 / nitrobenzene
View Scheme
参考文献
Kaiser; Schwartz; Colella; Wardell Jr.
Journal of Medicinal Chemistry, 1975 , vol. 18, # 7 p. 674 - 683
