2-(三甲基甲锡烷基)吡啶合成路线 （共 46 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 8 h; Heating;
参考文献
Heterocycles, , vol. 42, # 1 p. 189 - 194
反应条件
in benzene 0.5 h; Ambient temperature;
参考文献
Yamamoto; Ouchi; Tanaka
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 6 p. 1028 - 1030
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 5 h; Heating;
参考文献
Takahashi, Kazuko; Nihira, Takayasu
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 7 p. 1855 - 1859
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 23 h; Heating;
参考文献
Beley, Marc; Chodorowski, Sandrine; Collin, Jean-Paul; Sauvage, Jean-Pierre
Tetrahedron Letters, 1993 , vol. 34, # 18 p. 2933 - 2936
反应条件
tetrakis(triphenylphosphine) palladium(0) in xylene T=120°C; Stille coupling reaction; 12 h;
参考文献
Schwab, Peter F.H.; Fleischer, Frank; Michl, Josef
Journal of Organic Chemistry, 2002 , vol. 67, # 2 p. 443 - 449
反应条件
dinitrogen tetraoxide in tetrachloromethane; dimethyl sulfoxide T=20°C; Nitration; 16 h; dark;
参考文献
Fargeas, Valerie; Favresse, Fabien; Mathieu, Didier; Beaudet, Isabelle; Charrue, Pierre; Lebret, Bruno; Piteau, Marc; Quintard, Jean-Paul
European Journal of Organic Chemistry, 2003 , # 9 p. 1711 - 1721
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
12 h; Heating;
参考文献
Giuseppone, Nicolas; Schmitt, Jean-Louis; Lehn, Jean-Marie
Journal of the American Chemical Society, 2006 , vol. 128, # 51 p. 16748 - 16763
反应条件
1: 70 percent / Pd(PPh3)4 / toluene / 12 h / Heating
2: BBr3 / CH2Cl2 / 16 h / 25 °C
View Scheme
参考文献
Giuseppone, Nicolas; Schmitt, Jean-Louis; Lehn, Jean-Marie
Journal of the American Chemical Society, 2006 , vol. 128, # 51 p. 16748 - 16763
反应条件
1: 70 percent / Pd(PPh3)4 / toluene / 12 h / Heating
2: BBr3 / CH2Cl2 / 16 h / 25 °C
3: 12 mg / Dess-Martin reagent / CH2Cl2 / 6 h
View Scheme
参考文献
Giuseppone, Nicolas; Schmitt, Jean-Louis; Lehn, Jean-Marie
Journal of the American Chemical Society, 2006 , vol. 128, # 51 p. 16748 - 16763
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
16 h; Inert atmosphereReflux;
参考文献
Otsuki, Joe; Kurihara, Izumi; Imai, Arata; Hamada, Yuki; Omokawa, Nobuyuki
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 5 p. 902 - 909
