2-(三甲基甲锡烷基)吡啶合成路线 （共 46 条）
反应条件
1: 84 percent / (PPh3)2PdCl2 / m-xylene / 7 h / 135 °C
2: 92 percent / lithium aluminum hydride / tetrahydrofuran / 1.5 h / -78 - -20 °C
3: 66 percent / NBS; PPh3
View Scheme
参考文献
Kim, Minki; Kang, Chang Hoon; Hong, Subong; Lee, Won-Yong; Kim, Byeong Hyo
Inorganica Chimica Acta, 2013 , vol. 395, p. 145 - 150
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
Heating;
参考文献
Bailey, Thomas R.
Tetrahedron Letters, 1986 , vol. 27, # 37 p. 4407 - 4410
反应条件
tetrabutyl-ammonium chloride; palladium diacetate in N,N-dimethyl-formamide
T=115 - 120°C; Stille reaction; 3 h;
参考文献
Somei, Masanori; Sayama, Shinsuke; Naka, Katsumi; Shinmoto, Kotaro; Yamada, Fumio
Heterocycles, 2007 , vol. 73, # C p. 537 - 554
反应条件
tetrabutyl-ammonium chloride; palladium diacetate
参考文献
Somei, Masanori; Sayama, Shinsuke; Naka, Katsumi; Yamada, Fumio
Heterocycles, 1988 , vol. 27, # 7 p. 1585 - 1588
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
Stille coupling; 17 h; Heating;
参考文献
Fryatt, Tara; Pettersson, Hanna I.; Gardipee, Walter T.; Bray, Kurtis C.; Green, Stephen J.; Slawin, Alexandra M. Z.; Beall, Howard D.; Moody, Christopher J.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 7 p. 1667 - 1687
反应条件
bis-triphenylphosphine-palladium(II) chloride in m-xylene
10 h; Reflux;
参考文献
Kim, Minki; Kang, Chang Hoon; Hong, Subong; Lee, Won-Yong; Kim, Byeong Hyo
Inorganica Chimica Acta, 2013 , vol. 395, p. 145 - 150
