2-(二甲基氨基甲基)-5,6-二乙氧基-2,3-二氢茚-1-酮盐酸盐合成路线 （共 3 条）
反应条件
hydrogenchloride in ethanol
8 h; Heating;
参考文献
Daukshas, V. K.; Gaidyalis, P. G.; Labanauskas, L. K.; Gumbaragite, L. F.; Gasperavichene, G. A.
Pharmaceutical Chemistry Journal, 1991 , vol. 25, # 8 p. 544 - 547
Khimiko-Farmatsevticheskii Zhurnal, 1991 , vol. 25, # 8 p. 32 - 34
反应条件
1: 88 percent / pyridine, piperidine / 6 h / 110 °C
2: 95 percent / H2, Raney nickel, 15percent aq. KOH / 3 h / 60 °C / 68400.1 Torr
3: 70 percent / polyphosphoric acid / 0.33 h / 110 °C
4: 60 percent / conc. HCl / ethanol / 8 h / Heating
View Scheme
参考文献
Daukshas, V. K.; Gaidyalis, P. G.; Labanauskas, L. K.; Gumbaragite, L. F.; Gasperavichene, G. A.
Pharmaceutical Chemistry Journal, 1991 , vol. 25, # 8 p. 544 - 547
Khimiko-Farmatsevticheskii Zhurnal, 1991 , vol. 25, # 8 p. 32 - 34
反应条件
1: 70 percent / polyphosphoric acid / 0.33 h / 110 °C
2: 60 percent / conc. HCl / ethanol / 8 h / Heating
View Scheme
参考文献
Daukshas, V. K.; Gaidyalis, P. G.; Labanauskas, L. K.; Gumbaragite, L. F.; Gasperavichene, G. A.
Pharmaceutical Chemistry Journal, 1991 , vol. 25, # 8 p. 544 - 547
Khimiko-Farmatsevticheskii Zhurnal, 1991 , vol. 25, # 8 p. 32 - 34
