1,8-二乙酰基-3-羧基蒽醌合成路线 （共 17 条）
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine
参考文献
Gonnot, Vanessa; Tisserand, Steve; Nicolas, Marc; Baati, Rachid; Mioskowski, Charles
Tetrahedron Letters, 2007 , vol. 48, # 40 p. 7117 - 7119
反应条件
hydrogenchloride in water; acetone
参考文献
WO2004/50601 A2, ;
Page 6-7 ;
反应条件
anhydrous iron chloride T=65°C; 1.5 h;
参考文献
WO2009/90483 A1, ;
Page/Page column 9-10 ;
反应条件
sulfuric acid in ethanol; water; acetone pH=4.5 - 5;
参考文献
EP2196450 A1, ;
Page/Page column 6 ;
反应条件
1: 87 percent / K2CO3 / dimethylformamide / 12 h / 80 °C 2: 92 percent / Et3N; (dppf)PdCl2; dppf / dimethylformamide / 18 h / 80 °C / 750.06 Torr 3: KOH / methanol / 48 h / 60 °C 4: 414 mg / H2 / Pd/C / ethanol / 12 h / 20 °C / 750.06 Torr 5: 50 percent / AlCl3; NaCl / 2 h / 150 °C 6: 75 percent / Et3N / 1 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 25 p. 8982 - 8983
反应条件
1: 92 percent / Et3N; (dppf)PdCl2; dppf / dimethylformamide / 18 h / 80 °C / 750.06 Torr 2: KOH / methanol / 48 h / 60 °C 3: 414 mg / H2 / Pd/C / ethanol / 12 h / 20 °C / 750.06 Torr 4: 50 percent / AlCl3; NaCl / 2 h / 150 °C 5: 75 percent / Et3N / 1 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 25 p. 8982 - 8983
反应条件
1: KOH / methanol / 48 h / 60 °C 2: 414 mg / H2 / Pd/C / ethanol / 12 h / 20 °C / 750.06 Torr 3: 50 percent / AlCl3; NaCl / 2 h / 150 °C 4: 75 percent / Et3N / 1 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 25 p. 8982 - 8983
反应条件
1: 414 mg / H2 / Pd/C / ethanol / 12 h / 20 °C / 750.06 Torr 2: 50 percent / AlCl3; NaCl / 2 h / 150 °C 3: 75 percent / Et3N / 1 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 25 p. 8982 - 8983
