N,N-二甲基-1-(三甲基甲硅烷基)甲烷磺酰胺合成路线 (共 2 条)
反应条件
sodium hexamethyldisilazane 1) THF, room temp., 90 min., 2) room temp., 15 min.; Yield given. Multistep reaction;
参考文献
Mladenova, Margarita; Gaudemar-Bardone, Francoise
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 62, # 14 p. 257 - 268
反应条件
n-butyllithium; diisopropylamine
1) ether, hexane, -20 deg C, 1 h, 2) ether, 24 h, reflux; Yield given. Multistep reaction;
参考文献
Mladenova, Margarita; Gaudemar-Bardone, Francoise
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 62, # 14 p. 257 - 268