反应条件
1: diiodomethane; isopentyl nitrite / chloroform / 0.83 h / 80 °C / Inert atmosphere 2: palladium diacetate; sodium carbonate; triphenylphosphine / ethylene glycol dimethyl ether; water / 3 h / 100 °C / Inert atmosphere 3: hydrogenchloride / 1,4-dioxane / 5 h / Inert atmosphere; Reflux View Scheme
参考文献
Shi, Ce; Xiong, Zhengming; Chittepu, Padmaja; Aldrich, Courtney C.; Ohlfest, John R.; Ferguson, David M.
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 6 p. 501 - 504