1-甲基-3-(苯基甲基)-哌嗪(9ci)合成路线 （共 3 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
18 h; Heating;
参考文献
Ohnmacht, Cyrus J.; McLaren, Frances M.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1219 - 1224
反应条件
1: 89 percent / H2 / 10percent Pd-C / acetic acid / 6 h / 2585.7 Torr
2: 90 percent / LiAlH4 / tetrahydrofuran / 18 h / Heating
View Scheme
参考文献
Ohnmacht, Cyrus J.; McLaren, Frances M.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1219 - 1224
反应条件
1: dicyclohexylcarbodiimide, NEt3 / CH2Cl2 / 2.5 h / Ambient temperature
2: 89 percent / H2 / 10percent Pd-C / acetic acid / 6 h / 2585.7 Torr
3: 90 percent / LiAlH4 / tetrahydrofuran / 18 h / Heating
View Scheme
参考文献
Ohnmacht, Cyrus J.; McLaren, Frances M.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1219 - 1224
