1,5,6,7-四氢-4H-吲哚-4-酮合成路线 （共 29 条）
反应条件
1: H2 / Raney nickel / ethanol / 6 h / 60 - 70 °C / 2280 Torr 2: sodium methoxide / methanol 3: 75 percent / sodium metaperiodate / H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 581 - 588
反应条件
acetic acid; zinc Reflux;
参考文献
Spyridonidou, Katerina; Fousteris, Manolis; Antonia, Marazioti; Chatzianastasiou, Athanasia; Papapetropoulos, Andreas; Nikolaropoulos, Sotiris
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 16 p. 4810 - 4813
反应条件
1: conc. H2SO4 / ethyl acetate / 1 h 2: 96 percent / 29 percent aq. NH3 / ethanol / 12 h / 150 °C View Scheme
参考文献
Heterocycles, , vol. 22, # 10 p. 2313 - 2316
反应条件
anhydrous ammonium carbonate; hexan-1-ol T=120 - 130°C; 1 h;
参考文献
Berg, E. M. M. van den; Jansen, F. J. H. M.; Goede, A. T. J. W. de; Baldew, A. U.; Lugtenburg, J.
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, # 4 p. 287 - 297
反应条件
sodium hydride in N,N-dimethyl-formamide Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 1697 - 1702
反应条件
1: sodium methoxide / methanol 2: 75 percent / sodium metaperiodate / H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 581 - 588
反应条件
1: 1M H2SO4 / H2O / 3 h / Heating 2: 88 percent Chromat. / ammonium carbonate, 1-hexanol / 1 h / 120 - 130 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 109, # 4 p. 287 - 297
反应条件
sodium ethanolate; (NH4)2CO3 1.) electrolysis, EtOH, Pt-foil, 14 mA/Cm2, 80 min., R.T., 2.) MeOH, 150 degC, 40 h; Yield given. Multistep reaction;
参考文献
Chemistry Letters, , p. 1603 - 1604
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide T=90 - 92°C; 23 h;
参考文献
Laurila, Michael L.; Magnus, Nicholas A.; Staszak, Michael A.
Organic Process Research and Development, 2009 , vol. 13, # 6 p. 1199 - 1201
反应条件
1: 1) hydrazine monohydrate, 2) KOH / 1) ethylene glycol, 130 deg C, 2) 195 deg C, 3h 2: 1a) BuLi / 1a) THF, hexane, -70 deg C, 1b) 0 deg C, 1h, 2) THF, -40 deg C 3: molsieves (3 Angstroem), DDQ / toluene / Heating; one night 4: 89 percent Chromat. / 3M NaOH / ethanol / 1) 0 deg C, 2) r.t., 3h 5: 90 percent / transformed Escherichia coli cells View Scheme
参考文献
Berg, E. M. M. van den; Jansen, F. J. H. M.; Goede, A. T. J. W. de; Baldew, A. U.; Lugtenburg, J.
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, # 4 p. 287 - 297
