in further solvent(s) soln. NaBH4 in triglyme (tetraglyme) was added slowly for 2-3 h at roomtemp. to NaBF4 and AlCl3 in triglyme (tetraglyme); B2H6 was absorbed with THF;
参考文献
Kanth, Josyula V. B.; Brown, Herbert C.
Inorganic Chemistry, 2000 , vol. 39, # 8 p. 1795 - 1802
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反应条件
in neat (no solvent) byproducts: H2; (reactor of vac. vibratory ball mill type); vac. (molar ratio of LiBH4:NaBF4 = 4.2); IR-spectroscopy;
参考文献
Sov. J. Coord. Chem. (Engl. Transl.), , vol. 18, p. 429 - 434
Koordinatsionnaya Khimiya, , vol. 18, p. 497 - 502
in further solvent(s) soln. NaBH4 in triglyme (tetraglyme) was added slowly for 2-3 h at roomtemp. to NaBF4 and AlCl3 in triglyme (tetraglyme); B2H6 was absorbed with THF;
