in acetone under inert gas; dropwise addn. of p-MeOC6H4NC in acetone to a suspn. of the Pt complex in the presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in further solvent(s) soln. NaBH4 in triglyme (tetraglyme) was added slowly for 2-3 h at roomtemp. to NaBF4 and AlCl3 in triglyme (tetraglyme); B2H6 was absorbed with THF;
参考文献
Kanth, Josyula V. B.; Brown, Herbert C.
Inorganic Chemistry, 2000 , vol. 39, # 8 p. 1795 - 1802
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to a suspn. of the Pt complex in acetone in the presence of NaBF4 at room temp.; vigorous stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtrated, concd. to a small vol.; addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to a suspn. of the Pt complex in acetone in the presence of NaBF4 at room temp.; vigorous stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtrated, concd. to a small vol.; addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
in acetone under inert gas; dropwise addn. of the isocyanide in acetone to the suspn. of the Pd complex in acetone in presence of NaBF4 at room temp.; stirring for 1 h; solvent removed, residue dissolved in CH2Cl2; soln. filtered and concd., addn. of Et2O yields the solid; elem. anal.;
参考文献
Michelin, Rino A.; Zanotto, Livio; Braga, Dario; Sabatino, Piera; Angelici, Robert J.
Inorganic Chemistry, 1988 , vol. 27, p. 85 - 92
Meisters, M.; Moore, C. E.; Cassaretto, F. P.
Analytica Chimica Acta, 1969 , vol. 44, p. 287 - 291
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Gmelin Handbook: B: B-Verb.8, 11.2.3, page 167 - 173
