反应条件
in acetonitrile under Ar: addn. of Na(O2CMe) to soln. of (Mo(NO)2(MeCN)4)(BF4)2 in MeCN (stirred vigorously), stirred (2 h, room temp.); filtered, concd. (vac., 1/2 vol.), treated with CH2Cl2, white ppt. filtered off, filtrate treated with CH2Cl2, filtered, addn. of hexane, filtered, washed (hexane and CH2Cl2), dried (vac.), elem. anal.;
参考文献
Journal of molecular catalysis, , vol. 53, # 3 p. L9-L11
