in neat (no solvent) byproducts: carbon; violent react.;;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 1357 - 1358
Sc: MVol.C3, 6.2.2.1.8, page 38 - 38
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反应条件
oleic acid; 1-octadecene; oleylamine in neat (no solvent) (Ar); addn. of K compd. and Ho compd. to mixture of oleic acid, 1-octadecene, oleylamine at room temp., heating to 120°C under vacuum for30 min, heating to 250-330°C (22 K/min), storage at this temp. f or 15-120 min;
in hydrogenchloride byproducts: CO2; pH 1 to <4, heating to 60-100°C for 4h while stirring, washing with H2O until neutral react.;;
参考文献
Gmelin Handbook: Sc: MVol.C3, 6.2.2.1.3, page 35 - 36
Full Text Show Details
Th. Goldschmidt A.-G.
Patent: DE1169907 , 1964 ;
C. A., 1964 , vol. 61, p. 3965
in hydrogenchloride byproducts: CO2, CaCl2; pH 1 to <4, heating to 60-100°C for 4h while stirring, washing with H2O until neutral react.;;
参考文献
Gmelin Handbook: Sc: MVol.C3, 6.2.2.1.3, page 35 - 36
Full Text Show Details
Th. Goldschmidt A.-G.
Patent: DE1169907 , 1964 ;
C. A., 1964 , vol. 61, p. 3965
