in neat (no solvent) at room temp. in presence of moisture;;
参考文献
Popov, A. I.; Knudson, E. G.
Journal of the American Chemical Society, 1954 , vol. 76, p. 3921 - 3922
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Gmelin Handbook: Sc: MVol.C3, 6.2.2.1.8, page 38 - 38
in neat (no solvent) byproducts: carbon; violent react.;;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 1357 - 1358
Sc: MVol.C3, 6.2.2.1.8, page 38 - 38
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反应条件
oleic acid; 1-octadecene; oleylamine in neat (no solvent) (Ar); addn. of K compd. and Lu compd. to mixture of oleic acid, 1-octadecene, oleylamine at room temp., heating to 120°C under vacuum for30 min, heating to 250-330°C (22 K/min), storage at this temp. f or 15-120 min;
in gaseous matrix Irradiation (UV/VIS); laser ablation of metal, co-deposition with Ar or Ne containing CHF3 at 4 K, photolysis with Hg lamp (175 W); not isolated, detected by IR;
in gaseous matrix Irradiation (UV/VIS); laser ablation of metal, co-deposition with Ar or Ne containing CDF3 at 4 K, photolysis with Hg lamp (175 W); not isolated, detected by IR;
