in neat (no solvent) at room temp. in presence of moisture;;
参考文献
Popov, A. I.; Knudson, E. G.
Journal of the American Chemical Society, 1954 , vol. 76, p. 3921 - 3922
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Gmelin Handbook: Sc: MVol.C3, 6.2.2.1.8, page 38 - 38
in neat (no solvent) byproducts: (C6F5S)2, (C6F4S)2, (C6F4S)3; heated at 220°C under vac.; detd. by X-ray powder diffraction and mass spectrometry;
参考文献
Inorganic Chemistry, , vol. 41, # 1 p. 28 - 33
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反应条件
oleic acid; 1-octadecene; oleylamine in neat (no solvent) (Ar); addn. of K compd. and Er compd. to mixture of oleic acid, 1-octadecene, oleylamine at room temp., heating to 120°C under vacuum for30 min, heating to 250-330°C (22 K/min), storage at this temp. f or 15-120 min;
