3,5-二异丁基-4-(2-甲氧基苯甲酰基)-氧甲苯合成路线 （共 7 条）
反应条件
trifluoroacetic anhydride in benzene 23 h; Ambient temperature;
参考文献
Hattori; Hayashizaka; Miyano
Synthesis, 1995 , # 1 p. 41 - 43
反应条件
1: 96 percent / diethyl ether; benzene / from RT, 20 h, to reflux, 1 h 2: 100 percent / NaOCH3 / hexamethylphosphoric acid triamide; toluene / 1.5 h / Heating View Scheme
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
反应条件
1: 91 percent / diethyl ether; various solvent(s) / room temp., 17 h; reflux, 1 h 2: toluene; various solvent(s) / 2.5 h / Heating 3: H2O / ethanol / 0.5 h / Heating View Scheme
参考文献
Hattori; Hayashizaka; Miyano
Synthesis, 1995 , # 1 p. 41 - 43
反应条件
1: 91 percent / diethyl ether; various solvent(s) / room temp., 17 h; reflux, 1 h 2: toluene; various solvent(s) / 2.5 h / Heating View Scheme
参考文献
Hattori; Hayashizaka; Miyano
Synthesis, 1995 , # 1 p. 41 - 43
反应条件
1: 98 percent / diethyl ether; benzene / 1 h / Ambient temperature
2: 81 percent / acetic anhydride, aq. HI / 1 h / Heating
View Scheme
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
反应条件
1: 98 percent / diethyl ether; benzene / 1 h / Ambient temperature
2: 100 percent / NaOCH3 / hexamethylphosphoric acid triamide; toluene / 1.5 h / Heating
View Scheme
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
反应条件
1: 96 percent / diethyl ether; benzene / 1.) RT, 20 h, 2.) reflux, 1 h
2: 95 percent / NaOCH3 / hexamethylphosphoric acid triamide; toluene / 1.5 h / Heating
View Scheme
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
