anilinium hypophosphorous salt; triethylamine; tetrakis(triphenylphosphine) palladium(0) in acetonitrile 2 h; Heating;

1: With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; anilinium hypophosphite; triethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=120°C; Microwave irradiationInert atmosphere; 2: With sodium hydroxide in diethyl ether; water 3: With hydrogenchloride in water

water

1: phosphorus trichloride / 180 - 190 °C 2: water View Scheme

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potassium permanganate; water; potassium carbonate T=50°C; Bei 2.5 Monate langem Erwaermen;