1.1: 2,2,6,6-tetramethyl-piperidine / tert-butyl methyl ether / -5 - 0 °C / |Large scale 1.2: -5 - 0 °C / |Large scale 2.1: silica gel View Scheme
参考文献
Alorati, Anthony D.; Bio, Matthew M.; Brands, Karel M. J.; Cleator, Ed; Davies, Antony J.; Wilson, Robert D.; Wise, Chris S.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 637 - 641
1: With 2,2,6,6-tetramethyl-piperidine in tert-butyl methyl ether T=0°C; 2: With n-butyllithium in hexane; tert-butyl methyl ether T=0°C;
参考文献
Alorati, Anthony D.; Bio, Matthew M.; Brands, Karel M. J.; Cleator, Ed; Davies, Antony J.; Wilson, Robert D.; Wise, Chris S.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 637 - 641
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315