(S)-(-)-2-(二苯基磷酰)-2’-乙基-1,1’-联萘合成路线 （共 9 条）
参考文献
Takasago International Corporation
Patent: US5231202 A1, 1993 ;
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in diethyl ether 24 h; Heating;
参考文献
Uozumi, Yasuhiro; Hayashi, Tamio
Journal of the American Chemical Society, 1991 , vol. 113, # 26 p. 9887 - 9888
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in diethyl ether 24 h; Heating;
参考文献
Uozumi, Yasuhiro; Tanahashi, Asako; Lee, Sang-Yong; Hayashi, Tamio
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1945 - 1948
反应条件
1: 3N NaOH / dioxane; methanol 2: 81 percent / NiCl2(dppe) / diethyl ether / 24 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 113, # 26 p. 9887 - 9888
反应条件
1: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 2: 81 percent / NiCl2(dppe) / diethyl ether / 24 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1945 - 1948
反应条件
1: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 2: 81 percent / NiCl2(dppe) / diethyl ether / 24 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1945 - 1948
反应条件
1: 100 percent / pyridine / CH2Cl2 / 6 h / 0 °C 2: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 3: 81 percent / NiCl2(dppe) / diethyl ether / 24 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1945 - 1948
反应条件
trichlorosilane; triethylamine in xylene T=120°C; 3 h;
参考文献
Takasago International Corporation
Patent: US5231202 A1, 1993 ;
反应条件
trichlorosilane; triethylamine in xylene T=120°C; 3 h;
参考文献
Takasago International Corporation
Patent: US5231202 A1, 1993 ;
