反应条件
1.1: platinum(IV) oxide; hydrogen / tetrahydrofuran / 1 h / 24 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
2.2: 17 h / -78 - 0 °C / Inert atmosphere
3.1: AlCl3, aluminium chloride; ethane-1,2-dithiol / nitromethane / 0.5 h / -20 °C
View Scheme
参考文献
Fujiwara, Kenshu; Sato, Takuto; Sano, Yusuke; Norikura, Toshio; Katoono, Ryo; Suzuki, Takanori; Matsue, Hajime
Journal of Organic Chemistry, 2012 , vol. 77, # 11 p. 5161 - 5166