反应条件
1: (methoxycarbonylmethyl)methyldiphenylphosphonium chloride With potassium hexamethylsilazane in tetrahydrofuran Wittig reaction; 1 h; Inert atmosphere; 2: 2-chloro-benzaldehyde in tetrahydrofuran T=-78°C; Wittig reaction; Inert atmosphereCooling with acetone-dry ice; optical yield given as percent dediastereoselective reaction;
参考文献
Byrne, Peter A.; Gilheany, Declan G.
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9225 - 9239