3-苯甲酰基-2-苯并噁唑酮合成路线 (共 18 条)
反应条件
1-methyl-pyrrolidin-2-one; triethylamine 8 h; Ambient temperatureother time, other ratio of reactants; Product distribution;
参考文献
Ueda, Mitsuru; Mochizuki, Amane; Hiratsuka, Ichiro; Oikawa, Hideaki
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 11 p. 3291 - 3297
反应条件
in acetonitrile T=-12°C; also at room temp.; intermediate products, reaction half-lives studied; MechanismRate constant;
参考文献
Blonski, Casimir; Belghith, Hachemi; Klaebe, Alain; Perie, Jean-Jacques
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 1369 - 1374
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 1 h;
参考文献
Carato, Pascal; Yous, Said; Sellier, Didier; Poupaert, Jacques H.; Lebegue, Nicolas; Berthelot, Pascal
Tetrahedron, 2004 , vol. 60, # 45 p. 10321 - 10324
反应条件
bei der Destillation;
参考文献
Ransom
Chemische Berichte, 1898 , vol. 31, p. 1062,1065, 1268
American Chemical Journal, 1900 , vol. 23, p. 19
参考文献
Mustafa et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5121,5123
反应条件
1: 80 percent / AlCl3 / 3 h / 165 °C
2: 76 percent / K2CO3 / dimethylformamide / 2 h / 125 °C
View Scheme
参考文献
Ucar, Huseyin; Van Derpoorten, Kim; Cacciaguerra, Silvia; Spampinato, Santi; Stables, James P.; Depovere, Paul; Isa, Majed; Masereel, Bernard; Delarge, Jacques; Poupaert, Jacques H.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 7 p. 1138 - 1145
反应条件
PPA
Irradiationmicrowave (300 W), seven 30 sec-intervals over 15 min;
参考文献
Poupaert, Jacques H.; Depreux, Patrick; McCurdy, Christopher R.
Monatshefte fur Chemie, 2003 , vol. 134, # 6 p. 823 - 830
反应条件
in acetonitrile
48 h; Irradiation;
参考文献
Ishida,S. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 1135 - 1138