反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1: 100 percent / aq. Na<sub>2</sub>CO<sub>3</sub> / CHCl<sub>3</sub> / 3 h / 25 °C<br />2: 99 percent / LiBH<sub>4</sub> / tetrahydrofuran / 2 h / 25 °C<br />3: 97 percent / p-toluenesulfonic acid / acetone / 0.5 h / 25 °C<br />4: 92 percent / K<sub>2</sub>CO<sub>3</sub> / dimethylformamide / 10 h / 25 °C<br /> <br />
参考文献
Nicolaou; Snyder, Scott A.; Huang, Xianhai; Simonsen, Klaus B.; Koumbis, Alexandros E.; Bigot, Antony Journal of the American Chemical Society, 2004 , vol. 126, # 32 p. 10162 - 10173
