Bartlett, P. D.; Davis, R. E.
Journal of the American Chemical Society, 1958 , vol. 80, p. 2513 - 2516
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Gmelin Handbook: Na: SVol.4, 9, page 1387 - 1389
in carbon disulfide; tetrachloromethane byproducts: S7Cl2, S8Cl2, S9Cl2; dropwise addn. of a 4percent Cl2-soln. (0.094mol) in CCl4 to a soln. of 0.469mol S6 in CS2 at 0°C within 30min; warming to room temp.; furtherbyproducts;; concn. after 60min by evapn. at 20°C; filtration; removal of solvent; cooling at -35°C for several days; the viscous liquid was pipetted off from ppt. in the cold; mixt. obtained;;
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 41, # 8 p. 958 - 970