反应条件
1: 88 percent / iPr2EtN / CH2Cl2 2: K2CO3 / methanol 3: NBS / CH2Cl2 4: 86 percent / OsO4, N-methylmorpholine N-oxide / tetrahydrofuran; H2O 5: 97 percent / iPr2EtN / CH2Cl2 6: 79 percent / Zn, AcOH / ethanol 7: 86 percent / NaHCO3 / diphenyl ether / 0.5 h / 260 °C 8: Et3N, DMAP / CH2Cl2 / 0 °C 9: Bu3SnH, AIBN / benzene / 80 °C 10: 30percent H2O2, KHCO3 / methanol; tetrahydrofuran / Heating 11: 100 percent / imidazole / dimethylformamide 12: iPrEtN, DMAP / CH2Cl2 13: TBAF / tetrahydrofuran 14: SO3*Py, Et3N / dimethylsulfoxide 15: NaClO2, NaH2PO4*2H2O, 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O 16: CH2Cl2 17: 98 percent / AcCl / methanol 18: 96 percent / aq. 1 M NaOH / tetrahydrofuran; H2O View Scheme
