反应条件
1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / -20 °C 2: methanesulfonyl chloride; triethylamine / 0 °C / Reflux 3: hydrogenchloride / tetrahydrofuran 4: sodium hydrogencarbonate 5: triethylamine / 0 °C 6: sodium hydride / N,N-dimethyl-formamide 7: hydrogenchloride / methanol View Scheme
参考文献
Li, Ji; Feng, Yan Hua; Li, Xin Bai; Han, Wei; Liu, Huan Qiu; Shao, Guo Guang
Chinese Chemical Letters, 2012 , vol. 23, # 6 p. 647 - 649