in neat (no solvent) mixt. of metal and I2 was heated to the deflagration point of the mixt. in vac.; excess of I2 was evacuated, tube was filled with Ar, solidified metal part was removed, elem. anal.; metal triiodide was deposited on the wall of tube;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 628, # 3 p. 699 - 702
in neat (no solvent) Kinetics; byproducts: CO2, H2; passing gaseous mixt. of HI and CO (1:1, 10 l/h) over La2O3 at 473-973 Kfor 120 min; elem. anal. of samples;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 26, p. 1098 - 1099
Zhurnal Neorganicheskoi Khimii, , vol. 26, p. 2035 - 2038
in inert gas at 200-400°C; quant. reaction requires a tenfold excess of NH4I;
参考文献
Kiess, N. H.
Journal of Research of the National Bureau of Standards, Section A: Physics and Chemistry, 1963 , vol. 67, p. 343 - 345
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Gmelin Handbook: Sc: MVol.C1, 2.4.3.3.9.7, page 215 - 216
