(3-氨丙基)三甲氧基硅烷合成路线 （共 22 条）
反应条件
1: T=130°C; 6 h; 2: With ethylenediamine T=110°C; 0.05 h;
参考文献
US2012/71650 A1, ;
Page/Page column 8 ;
反应条件
methanol T=20°C; 0.5 h;
参考文献
WACKER CHEMIE AG
Patent: US2011/282088 A1, 2011 ;
Location in patent: Page/Page column 5 ;
反应条件
bis-trimethylsilyl ether
参考文献
Lukasiak,J. et al.
Roczniki Chemii, 1973 , vol. 47, p. 1975 - 1976
反应条件
hypophosphorous ether; trifluoroacetic acid in acetonitrile 3 h; Heating;
参考文献
Deprele, Sylvine; Montchamp, Jean-Luc
Journal of Organometalic Chemistry, 2002 , vol. 643-644, p. 154 - 163
反应条件
1: With sodium methylate T=50°C; 2 h; 2: With formic acid T=135 - 210°C; P=10 - 760.051 Torr; 2.16667 h; Product distribution / selectivity;
参考文献
Childress, R. Shawn; McIntyre, James L.
Patent: US2006/235221 A1, 2006 ;
Location in patent: Page/Page column 4 ;
反应条件
sodium ethanolate in ethanol T=80°C; 3.25 h; Conversion of starting material;
参考文献
General Electric Company
Patent: US6673954 B1, 2004 ;
Location in patent: Page column 8 ;
反应条件
2,2'-dimorpholinodiethyl ether in ethyl acetate T=0 - 10°C;
参考文献
MOMENTIVE PERFORMANCE MATERIALS GMBH; SIMANDAN, Tiberiu, L.; WAGNER, Roland; GLATZER, Holger, J.; SOCKEL, Karl-Heinz; STACHULLA, Karl-Heinz; WENSKE, Christian
Patent: WO2013/181136 A1, 2013 ;
Location in patent: Page/Page column 25-26 ;
反应条件
triethylamine in acetonitrile T=80°C; 15 h;
参考文献
Coll, Carmen; Aznar, Elena; Martinez-Manez, Ramon; Marcos, M. Dolores; Sancenon, Felix; Soto, Juan; Amoros, Pedro; Cano, Joan; Ruiz, Eliseo
Chemistry - A European Journal, 2010 , vol. 16, # 33 p. 10048 - 10061
反应条件
in methanol; water Si-compd. dissoln. in MeOH, aq. soln. of NaOH addn., refluxing (1 h), soln. of Cu-compd. in MeOH addn., refluxing (30 min), MeOH distillation off with simultaneous addn. of EtOH; NaCl filtration off, solvent removing; elem. anal.;
参考文献
Russian Chemical Bulletin, , vol. 47, # 12 p. 2448 - 2450
反应条件
1: gamma-aminopropyl trimethoxy silane With hypophosphorous ether; trifluoroacetic acid in acetonitrile
2 h; Heating;
2: cyclohexene With triethyl borane in hexane; acetonitrile
T=20°C; 2 h;
参考文献
Deprele, Sylvine; Montchamp, Jean-Luc
Journal of Organometalic Chemistry, 2002 , vol. 643-644, p. 154 - 163
