4-(2,2:6,2-四吡啶-4-基)苯甲醛合成路线 （共 6 条）
反应条件
calcium carbonate in 1,4-dioxane; water 30 h; Reflux;
参考文献
Bhaumik, Chanchal; Das, Shyamal; Saha, Debasish; Dutta, Supriya; Baitalik, Sujoy
Inorganic Chemistry, 2010 , vol. 49, # 11 p. 5049 - 5062
反应条件
1: With N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 24 h; Inert atmosphereReflux; 2: With calcium carbonate in 1,4-dioxane; water 24 h; Reflux;
参考文献
Tan, Yiqun; Liu, Min; Gao, Junkuo; Yu, Jiancan; Cui, Yuanjing; Yang, Yu; Qian, Guodong
Dalton Transactions, 2014 , vol. 43, # 21 p. 8048 - 8053
反应条件
ammonia; potassium hydroxide in ethanol; water T=20°C; 8 h;
参考文献
Patel, Mohan N.; Joshi, Hardik N.; Patel, Chintan R.
Polyhedron, 2012 , vol. 40, # 1 p. 159 - 167
反应条件
1: potassium tert-butylate / tetrahydrofuran 2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane 3: 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane View Scheme
参考文献
Tan, Yiqun; Liu, Min; Gao, Junkuo; Yu, Jiancan; Cui, Yuanjing; Yang, Yu; Qian, Guodong
Dalton Transactions, 2014 , vol. 43, # 21 p. 8048 - 8053
反应条件
1: potassium tert-butylate / tetrahydrofuran 2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane 3: 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane View Scheme
参考文献
Tan, Yiqun; Liu, Min; Gao, Junkuo; Yu, Jiancan; Cui, Yuanjing; Yang, Yu; Qian, Guodong
Dalton Transactions, 2014 , vol. 43, # 21 p. 8048 - 8053
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran Suzuki cross-coupling reaction; Heating;
参考文献
Goodall, Wendy; Wild, Kerstin; Arm, Kathryn J.; Williams, J.A. Gareth
Journal of the Chemical Society. Perkin Transactions 2, 2002 , # 10 p. 1669 - 1681
