反应条件
1: 4,6-dichloro-2-iodo-3-methoxyphenol; (S)-(-)-1-ethyl-2-aminomethylpyrrolidine With triethylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran sealed tubeInert atmosphere; 2: molybdenum hexacarbonate With pyridine in tetrahydrofuran T=70°C; 19 h; sealed tubeInert atmosphere;
参考文献
AARHUS UNIVERSITET; SKRYDSTRUP, Troels; LINDHARDT, Anders Thyboe; HERMANGE, Philippe; TAANING, Rolf Hejle; FRIIS, Stig Duering
Patent: WO2012/79583 A1, 2012 ;
Location in patent: Page/Page column 95; 96 ;