in tetrachloromethane
thermolysis at 70.4°C in the absence of O2; detected by NMR;
参考文献
Muller, E. F.; Hyne, J. B.
Journal of the American Chemical Society, 1969 , vol. 91, p. 1907 - 1912
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Gmelin Handbook: S: SVol.4a/b, 2.3.3.1, page 435 - 436
mercury in tetrachloromethane
in dry CCl4 at room temp.;
参考文献
Murthy, A. R. V.
Proceedings - Indian Academy of Sciences, Section A, 1953 , vol. 37, p. 23 - 28
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Gmelin Handbook: S: SVol.4a/b, 1.1.4.2, page 18 - 18
Muller, E. F.; Hyne, J. B.
Journal of the American Chemical Society, 1969 , vol. 91, p. 1907 - 1912
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Gmelin Handbook: S: SVol.4a/b, 4.1.3.4, page 460 - 461
in neat (no solvent)
vac.-distn. of H2S3, 20 Torr, glycerine bath 100°C;; one third reacts to H2S2, one third distilles without decompn., one third decomposes into H2S and S;;
