2,2-二甲基-1-(2-硫酮-3-噻唑烷基)-1-丙酮合成路线 （共 9 条）
反应条件
T=75°C; Rate constant;
参考文献
Yamada, Shinji
Angewandte Chemie, 1993 , vol. 105, # 7 p. 1128 - 1130
反应条件
1: 83 percent / tetrahydrofuran / 24 h / 80 °C 2: 93 percent / K2CO3 / acetone / 24 h / 40 °C View Scheme
参考文献
Dai, Wei-Min; Cheung, Yuk King; Tang, Kit Wan; Choi, Pui Yiu; Chung, Suet Lam
Tetrahedron, 1995 , vol. 51, # 45 p. 12263 - 12276
反应条件
sodium hydride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Yamada, Shinji
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1591 - 1592
反应条件
in toluene T=65°C; 65 h; other diols and acylating agents; Product distribution;
参考文献
Yamada, Shinji; Sugaki, Takayuki; Matsuzaki, Kazuhiro
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 5932 - 5938
反应条件
sodium hydride in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Dai, Wei-Min; Cheung, Yuk King; Tang, Kit Wan; Choi, Pui Yiu; Chung, Suet Lam
Tetrahedron, 1995 , vol. 51, # 45 p. 12263 - 12276
反应条件
zinc in tetrahydrofuran 1) 30 deg C, 2 h, 2) reflux, 18 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 3 p. 793 - 794
反应条件
in tetrahydrofuran
T=80°C; 12 h;
参考文献
Dai, Wei-Min; Cheung, Yuk King; Tang, Kit Wan; Choi, Pui Yiu; Chung, Suet Lam
Tetrahedron, 1995 , vol. 51, # 45 p. 12263 - 12276
反应条件
in toluene
T=100°C; 40 h;
参考文献
Hornberger, Keith R.; Badiang, Jennifer G.; Salovich, James M.; Kuntz, Kevin W.; Emmitte, Kyle A.; Cheung, Mui
Tetrahedron Letters, 2008 , vol. 49, # 44 p. 6348 - 6351
反应条件
in toluene
T=80°C; 18 h;
参考文献
Yamada, Shinji; Sugaki, Takayuki; Matsuzaki, Kazuhiro
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 5932 - 5938
