(3beta)-24-溴-3-[(叔-丁基)二甲基硅烷基氧基]-胆-5-烯合成路线 （共 2 条）
反应条件
With 1H-imidazole; carbon tetrabromide; triphenylphosphine in diethyl ether; acetonitrile T=0 - 20°C; Inert atmosphere; Show Experimental Procedure
参考文献
Johnston, Jonathan B.; Singh, Arti A.; Clary, Anaelle A.; Chen, Chiung-Kuan; Hayes, Patricia Y.; Chow, Sharon; De Voss, James J.; Ortiz De Montellano, Paul R. Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 13 p. 4064 - 4081
反应条件
Multi-step reaction with 2 steps 1: acetone / 23 h / 20 °C / Inert atmosphere2: N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere
参考文献
Johnston, Jonathan B.; Singh, Arti A.; Clary, Anaelle A.; Chen, Chiung-Kuan; Hayes, Patricia Y.; Chow, Sharon; De Voss, James J.; Ortiz De Montellano, Paul R. Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 13 p. 4064 - 4081
