N-二乙基氨基-N-氧代亚硝酰胺钠盐合成路线 （共 7 条）
反应条件
HOCbl*HCl in water T=25°C; pH=10.8; aq. bufferInert atmosphere; Kinetics; pH-valueReagent/catalystTemperatureTime;
参考文献
Hassanin, Hanaa A.; Hannibal, Luciana; Jacobsen, Donald W.; El-Shahat, Mohamed F.; Hamza, Mohamed S. A.; Brasch, Nicola E.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 47 p. 8909 - 8913
反应条件
in N,N-dimethyl-formamide Ambient temperature;
参考文献
Saavedra, Joseph E.; Dunams, Tambra M.; Flippen-Anderson, Judith L.; Keefer, Larry K.
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6134 - 6138
反应条件
15-crown-5 in sulfolane T=0°C; 1 h; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 13 p. 3961 - 3970
反应条件
in N,N-dimethyl-formamide Ambient temperature;
参考文献
Saavedra, Joseph E.; Dunams, Tambra M.; Flippen-Anderson, Judith L.; Keefer, Larry K.
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6134 - 6138
参考文献
Saavedra, Joseph E.; Dunams, Tambra M.; Flippen-Anderson, Judith L.; Keefer, Larry K.
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6134 - 6138
反应条件
HOCbl*HCl in water T=25°C; pH=10.8; aq. bufferInert atmosphere; Kinetics; pH-valueReagent/catalystTemperatureTime;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 47 p. 8909 - 8913
反应条件
nitrogen(II) oxide; sodium methylate in methanol; diethyl ether
T=20°C; P=2068.65 Torr; 24 h;
参考文献
THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY, DEPARTMENT OF HEALTH AND HUMAN SERVICES; THE ARIZONA BOARD OF REGENTS, ON BEHALF OF THE UNIVERSITY OF ARIZONA; MIRANDA, Katrina M.; WINK, David A.; SALMON, Debra J.; BASUDHAR, Debashree; KEEFER, Larry K.; SAAVEDRA, Joseph E.; ANDREI, Daniela
Patent: WO2011/116336 A1, 2011 ;
Location in patent: Page/Page column 35-36 ;
WO 2011/116336 A1
