2-碘-34-二甲氧基苯甲醛合成路线 （共 15 条）
反应条件
sodium hydride; triphenylphosphine; zinc; NiCl2((PPh3)P)2 in toluene T=90 - 95°C; Ullmann-type coupling reaction; 4 h; Product distribution; Further Variations:Reagentsreaction time;
参考文献
Hong; Hoen; Zhang; Lin
Synlett, 2001 , # 10 p. 1527 - 1530
参考文献
Nilsson
Acta Chemica Scandinavica (1947-1973), 1958 , vol. 12, p. 1830,1832
反应条件
1: 40 percent / cuprous iodide / various solvent(s) / 4 h / 175 °C 2: 87 percent / sodium borohydride / tetrahydrofuran; H2O / 2.5 h / 40 °C View Scheme
参考文献
Markovich; Tantishaiyakul; Hamada; Miller; Romstedt; Shams; Shin; Fraundorfer; Doyle; Feller
Journal of Medicinal Chemistry, 1992 , vol. 35, # 3 p. 466 - 479
反应条件
copper(l) iodide in various solvent(s) T=175°C; 4 h;
参考文献
Markovich; Tantishaiyakul; Hamada; Miller; Romstedt; Shams; Shin; Fraundorfer; Doyle; Feller
Journal of Medicinal Chemistry, 1992 , vol. 35, # 3 p. 466 - 479
反应条件
potassium permanganate
参考文献
Manske et al.
Canadian Journal of Chemistry, 1951 , vol. 29, p. 526,532
