4-溴甲基苯硼酸频哪醇酯合成路线 (共 29 条)
反应条件
in N,N-dimethyl-formamide T=20°C; Substitution; 24 h;
参考文献
Ramalingam, Kondareddiar; Nowotnik, David P.
Organic Preparations and Procedures International, 1991 , vol. 23, # 6 p. 729 - 734
反应条件
1: 90 percent / acetone / 12 h / Heating 2: 73 percent / NH2NH2*H2O / methanol / 12 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 6 p. 729 - 734
反应条件
potassium carbonate in acetone 12 h; Heating / reflux;
参考文献
RATIOPHARM GMBH
Patent: WO2006/81807 A2, 2006 ;
Location in patent: Page/Page column 20; 32 ;
反应条件
in acetone Condensation; 12 h; Heating;
参考文献
Ramalingam, Kondareddiar; Nowotnik, David P.
Organic Preparations and Procedures International, 1991 , vol. 23, # 6 p. 729 - 734
反应条件
1: 82 percent / K2CO3 / dimethylformamide / 3 h / 80 °C 2: 90 percent / pyridine / CH2Cl2 / 0 °C 3: 80 percent / aq. Na2CO3 / Pd(PPh3)4 / toluene / 10 h / 80 °C 4: aq. NaOH / methanol / 1 h / Heating 5: 92 mg / aq. NaOH / methanol / 8 h / Heating View Scheme
参考文献
Zhang, Chen; Zheng, Guojun; Fang, Lijing; Li, Yulin
Synlett, 2006 , # 3 p. 475 - 477
反应条件
1: 53 percent / dimethylformamide / 24 h / 20 °C 2: 87 percent / H2; NH3 / 5 percent Rh/Al / ethanol / 24 h / 2585.74 Torr View Scheme
参考文献
Ramalingam, Kondareddiar; Nowotnik, David P.
Organic Preparations and Procedures International, 1991 , vol. 23, # 6 p. 729 - 734
反应条件
sodium azide in ethanol T=20°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 51, # 30 p. 3913 - 3917
反应条件
in acetonitrile T=85°C; 12 h;
参考文献
Morrison, Daniel E.; Issa, Fatiah; Bhadbhade, Mohan; Groebler, Ludwig; Witting, Paul K.; Kassiou, Michael; Rutledge, Peter J.; Rendina, Louis M.
Journal of Biological Inorganic Chemistry, 2010 , vol. 15, # 8 p. 1305 - 1318
反应条件
triphenylphosphine hydrobromide in acetonitrile T=90°C; 6 h;
参考文献
Das, Bhaskar C.; Zhao, Xiaoping; Tang, Xiang-Ying; Yang, Fajun
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 18 p. 5638 - 5641