4-邻苯二甲酰亚氨基甲基苯基硼酸频哪醇酯合成路线 （共 9 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 72 h; Solvent;
参考文献
Chung, Sheng-Hsuan; Lin, Ting-Ju; Hu, Qian-Yu; Tsai, Chia-Hua; Pan, Po-Shen
Molecules, 2013 , vol. 18, # 10 p. 12346 - 12367
反应条件
potassium carbonate in acetone 12 h; Heating / reflux;
参考文献
RATIOPHARM GMBH
Patent: WO2006/81807 A2, 2006 ;
Location in patent: Page/Page column 20; 32 ;
反应条件
in acetone Condensation; 12 h; Heating;
参考文献
Ramalingam, Kondareddiar; Nowotnik, David P.
Organic Preparations and Procedures International, 1991 , vol. 23, # 6 p. 729 - 734
反应条件
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / |Inert atmosphere 2: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
1: magnesium sulfate / methanol / 6 h / 20 °C 2: sodium tetrahydroborate / 5 h / 20 °C 3: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / |Inert atmosphere 4: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
1: sodium tetrahydroborate / 5 h / 20 °C 2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / |Inert atmosphere 3: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
1: magnesium sulfate / methanol / 6 h / 20 °C 2: sodium tetrahydroborate / 5 h / 20 °C 3: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / |Inert atmosphere 4: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
1: 52 percent / hexane / 24 h / 20 °C 2: 90 percent / acetone / 12 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 6 p. 729 - 734
反应条件
hydrazine hydrate in tetrahydrofuran 12 h; Reflux; Solvent;
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
