1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C 2: triethylamine / dichloromethane / 2.5 h / 20 °C View Scheme
参考文献
Park, HoonGyu; Kim, Bojung; Bae, Daeil; Lim, Byungjo; Ko, Misun; Oh, Sehan; Kim, Hakwon
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 4 p. 1389 - 1392
1.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C 2.1: triethylamine / dichloromethane / 2.5 h / 20 °C 3.1: sodium azide / N,N-dimethyl-formamide / 3.5 h / 80 °C 4.1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C / 9000.9 Torr 5.1: (2R,3R)-(-)-di-O-(p-toluoyl)-tartaric acid / dimethyl sulfoxide / 3 h / 20 °C / Resolution of racemate 5.2: 1 h / 20 °C View Scheme
参考文献
Park, HoonGyu; Kim, Bojung; Bae, Daeil; Lim, Byungjo; Ko, Misun; Oh, Sehan; Kim, Hakwon
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 4 p. 1389 - 1392
1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C 2: triethylamine / dichloromethane / 2.5 h / 20 °C 3: sodium azide / N,N-dimethyl-formamide / 3.5 h / 80 °C 4: palladium 10 on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C / 9000.9 Torr 5: pyridine / ethyl acetate / 1 h / 20 °C View Scheme
参考文献
Park, HoonGyu; Kim, Bojung; Bae, Daeil; Lim, Byungjo; Ko, Misun; Oh, Sehan; Kim, Hakwon
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 4 p. 1389 - 1392
