N,N-二甲基苯并恶唑-2-胺合成路线 (共 19 条)
反应条件
1H-imidazole; anhydrous iron chloride T=130°C; 12 h;
参考文献
Wang, Jian; Hou, Ji-Ting; Wen, Jun; Zhang, Ji; Yu, Xiao-Qi
Chemical Communications, 2011 , vol. 47, # 12 p. 3652 - 3654
反应条件
potassium dichromate; [Pd(2,2'-bipyridine)Cl2]; copper (I) cyanide; potassium carbonate in chlorobenzene T=150°C; 24 h; Sealed tubeMolecular sieve; Catalytic behavior; SolventReagent/catalyst;
参考文献
Chen, Shuyou; Zheng, Kui; Chen, Fan
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6297 - 6299,3
反应条件
in tetrahydrofuran T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286
反应条件
in water T=20°C; 1 h;
参考文献
Robin, Maxime; Faure, Robert; Perichaud, Alain; Galy, Jean-Pierre
Synthetic Communications, 2002 , vol. 32, # 7 p. 981 - 988
反应条件
1: With triethylamine in chloroform T=-30 - -20°C; 2: With silica gel in chloroform T=20°C; 1.5 h;
参考文献
Ohno, Kosei; Ishida, Wakako; Kamata, Kazuyuki; Oda, Kazuaki; Machida, Minoru
Heterocycles, 2003 , vol. 59, # 1 p. 317 - 322
反应条件
1: N,N-dimethyl-formamide With ammonia in water T=240°C; 0.666667 h; 2: 2-chloro-benzoxazole in water T=30°C; 0.333333 h;
参考文献
Petersen, Trine P.; Larsen, Anders Foller; Ritzen, Andreas; Ulven, Trond
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4190 - 4195
反应条件
in tetrahydrofuran T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286
反应条件
1H-imidazole; anhydrous iron chloride T=130°C; 12 h;
参考文献
Wang, Jian; Hou, Ji-Ting; Wen, Jun; Zhang, Ji; Yu, Xiao-Qi
Chemical Communications, 2011 , vol. 47, # 12 p. 3652 - 3654
反应条件
triethylamine in N,N-dimethyl-formamide 24 h; Heating;
参考文献
El-Faham, Ayman; Chebbo, Mohamed; Abdul-Ghani, Mohamed; Younes, Ghassan
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 3 p. 599 - 606
反应条件
in tetrahydrofuran T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286