iodine in cyclohexane 24 h; Irradiation;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3903207', constants.ctx, '0')">titanium tetrachloride</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '8973685', constants.ctx, '0')">zinc</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />&nbsp;Heating;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: 75 percent / toluene / 3 h / 80 &deg;C<br />2.1: n-BuLi / hexane; tetrahydrofuran / 2 h / 20 &deg;C<br />2.2: tetrahydrofuran; hexane / 3 h / 20 &deg;C<br />2.3: 49 percent / TeCl₄; tellurium / CHCl₃ / 5 h / 20 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: hexane; tetrahydrofuran / 3 h / 0 - 20 &deg;C / |Inert atmosphere; |Schlenk technique<br />2: [RhCl(η²:η²-cycloocta-1,5-diene)]2; 2,4-dimethylpentan-3-one / hexane; tetrahydrofuran / 24 h / 60 &deg;C / |Inert atmosphere; |Schlenk technique<br /> <br /> &nbsp;