in tetrahydrofuran
byproducts: N2; High Pressure; AgN3 loaded into reactor with solvent, pressurized to 1 atm with N2, heated to 130°C and held overnight, then raised to 200°C and held for 1 d; filtration, washing, drying under vac.;
参考文献
Grocholl, Luke; Wang, Jianjun; Gillan, Edward G.
Materials Research Bulletin, 2003 , vol. 38, # 2 p. 213 - 220
in toluene
byproducts: N2; High Pressure; AgN3 loaded into reactor with solvent, pressurized to 1 atm with N2, heated to 130°C and held overnight, then raised to 200°C and held for 1 d; filtration, washing, drying under vac.;
参考文献
Grocholl, Luke; Wang, Jianjun; Gillan, Edward G.
Materials Research Bulletin, 2003 , vol. 38, # 2 p. 213 - 220
